The 8 references with contexts in paper A. Osipov S., E. Nechaeva B., L. Truhacheva A., А. Осипов С., Е. Нечаева Б., Л. Трухачева А. (2018) “Применение хроматографической колонки с нитрильным сорбентом для анализа гидроксикарбамида методом хроматографии гидрофильных взаимодействий // Chromatographic column with nitrile sorbent USED in the analysis of hydroxycarbamide by hydrophilic interaction liquid chromatography” / spz:neicon:vedomostincesmp:y:2016:i:3:p:58-61

1
British Pharmacopoeia 2012. Monograph: Hydroxycarbamide Capsules.
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    Ïðåïàðàò îïèñàí â âåäóùèõ çàðóáåæíûõ ôàðìàêîïåÿõ.ÑðåäèçàðåãèñòðèðîâàííûõâÐîññèéñêîéÔåäåðàöèè ëåêàðñòâåííûõ ïðåïàðàòîâ äëÿ êîëè÷åñòâåííîãî îïðåäåëåíèÿ ãèäðîêñèêàðáàìèäà (ÃÊ) íàèáîëåå ÷àñòî ïðèìåíÿþò ìåòîä âûñîêîýôôåêòèâíîé æèäêîñòíîéõðîìàòîãðàôèè(ÂÝÆÕ),ïðèâåäåííûéâÁðèòàíñêîé ôàðìàêîïåå
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    . Õðîìàòîãðàôèðîâàíèå ïðîâîäÿò íà êîëîíêàõ ñ ñîðáåíòàìè Ñ18, â êà÷åñòâå ïîäâèæíîéôàçûèñïîëüçóþòâîäó.Âôàðìàêîïåéíîé ñòàòüå äëÿ àíàëèçà ïðåïàðàòîâ à Êðåêîìåíäîâàíî èñïîëüçîâàòü õðîìàòîãðàôè÷åñêóþ êîëîíêó Spherisorb ODS2 250 ́4,6 ìì.

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European Pharmacopoeia. Edition 8.0. Monograph : Hydroxycarbamide.
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    Õðîìàòîãðàôèðîâàíèå ïðîâîäÿò íà êîëîíêàõ ñ ñîðáåíòàìè Ñ18, â êà÷åñòâå ïîäâèæíîéôàçûèñïîëüçóþòâîäó.Âôàðìàêîïåéíîé ñòàòüå äëÿ àíàëèçà ïðåïàðàòîâ à Êðåêîìåíäîâàíî èñïîëüçîâàòü õðîìàòîãðàôè÷åñêóþ êîëîíêó Spherisorb ODS2 250 ́4,6 ìì. Òàêæå èñïîëüçóåòñÿ ìåòîäèêà Åâðîïåéñêîé ôàðìàêîïåè
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    äëÿ êîëè÷åñòâåííîãî îïðåäåëåíèÿ è îïðåäåëåíèÿ ïðèìåñåé (èíûõ, ÷åì ìî÷åâèíà) â ñóáñòàíöèè ÃÊ. Õðîìàòîãðàôèðîâàíèå ïðîâîäÿò òàêæå íà êîëîíêàõ Ñ18, â êà÷åñòâå ïîäâèæíîé ôàçû ïðèìåíÿþò ñìåñü ìåòàíîëà è âîäû (5:95).

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The United States Pharmacopoeia 38. Monograph: Hydroxyurea.
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    Òàêæå èñïîëüçóåòñÿ ìåòîäèêà Åâðîïåéñêîé ôàðìàêîïåè [2] äëÿ êîëè÷åñòâåííîãî îïðåäåëåíèÿ è îïðåäåëåíèÿ ïðèìåñåé (èíûõ, ÷åì ìî÷åâèíà) â ñóáñòàíöèè ÃÊ. Õðîìàòîãðàôèðîâàíèå ïðîâîäÿò òàêæå íà êîëîíêàõ Ñ18, â êà÷åñòâå ïîäâèæíîé ôàçû ïðèìåíÿþò ñìåñü ìåòàíîëà è âîäû (5:95). ÂÔàðìàêîïååÑØÀ
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    äëÿêîëè÷åñòâåííîãîîïðåäåëåíèÿ à Êâ ñóáñòàíöèè è ëåêàðñòâåííîé ôîðìå (êàïñóëû) èñïîëüçóþò èîí-ïàðíóþ õðîìàòîãðàôèþ íàêîëîíêàõÑ18(ïîäâèæíàÿôàçà—ñìåñüáóôåðíîãî ðàñòâîðà ñ òåòðàáóòèëàììîíèÿ ãèäðîñóëüôàòîì (pH 5,0) è ìåòàíîëà (85:15)).

4
The United States Pharmacopoeia 38. Monograph: Hydroxyurea Capsules.
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    Òàêæå èñïîëüçóåòñÿ ìåòîäèêà Åâðîïåéñêîé ôàðìàêîïåè [2] äëÿ êîëè÷åñòâåííîãî îïðåäåëåíèÿ è îïðåäåëåíèÿ ïðèìåñåé (èíûõ, ÷åì ìî÷åâèíà) â ñóáñòàíöèè ÃÊ. Õðîìàòîãðàôèðîâàíèå ïðîâîäÿò òàêæå íà êîëîíêàõ Ñ18, â êà÷åñòâå ïîäâèæíîé ôàçû ïðèìåíÿþò ñìåñü ìåòàíîëà è âîäû (5:95). ÂÔàðìàêîïååÑØÀ
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    äëÿêîëè÷åñòâåííîãîîïðåäåëåíèÿ à Êâ ñóáñòàíöèè è ëåêàðñòâåííîé ôîðìå (êàïñóëû) èñïîëüçóþò èîí-ïàðíóþ õðîìàòîãðàôèþ íàêîëîíêàõÑ18(ïîäâèæíàÿôàçà—ñìåñüáóôåðíîãî ðàñòâîðà ñ òåòðàáóòèëàììîíèÿ ãèäðîñóëüôàòîì (pH 5,0) è ìåòàíîëà (85:15)).

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    Äëÿ îïðåäåëåíèÿ ìî÷åâèíû â ñóáñòàíöèè à Êïî Ôàðìàêîïåå ÑØÀ ïðèìåíÿþò íèñõîäÿùóþ õðîìàòîãðàôèþ íà áóìàãå (Whatman ¹ 1). Ñëåäóåò îòìåòèòü, ÷òîäàííûéìåòîäâåñüìàäëèòåëåíèòðóäîåìîê.Âñîîòâåòñòâóþùåé ìîíîãðàôèè Ôàðìàêîïåè ÑØÀ ñîäåðæàíèå ìî÷åâèíû â êàïñóëàõ ïðåïàðàòà íå ðåãëàìåíòèðîâàíî
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    . Ïðèìåíåíèå ìåòîäà ÂÝÆÕ äëÿ ðàçäåëåíèÿ à Êè ìî÷åâèíû â çàðóáåæíûõ ôàðìàêîïåÿõ íåîïèñàíî.Íåîáõîäèìîîòìåòèòü,÷òîâóñëîâèÿõîáðàùåííî-ôàçîâîé õðîìàòîãðàôèè à Êè ìî÷åâèíà íå ðàçäåëÿþòñÿ. Ðàíåå áûëà ïîêàçàíà âîçìîæíîñòü ïðèìåíåíèÿ õðîìàòîãðàôè÷åñêèõ êîëîíîê ñ àìèíî- è äèîëüíûìè ñîðáåíòàìè äëÿ ðàçäåëåíèÿ ñìåñåé à Êè ìî÷åâèíû [5].

5
Osipov AS, Nechaeva EB, Pobedin OA. The use of hydrophilic interaction liquid chromatography for analysis of hydroxyurea. Razrabotka i registratsiya lekarstvennyh sredstv 2015; (2): 140–4 (in Russian).
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    Ïðèìåíåíèå ìåòîäà ÂÝÆÕ äëÿ ðàçäåëåíèÿ à Êè ìî÷åâèíû â çàðóáåæíûõ ôàðìàêîïåÿõ íåîïèñàíî.Íåîáõîäèìîîòìåòèòü,÷òîâóñëîâèÿõîáðàùåííî-ôàçîâîé õðîìàòîãðàôèè à Êè ìî÷åâèíà íå ðàçäåëÿþòñÿ. Ðàíåå áûëà ïîêàçàíà âîçìîæíîñòü ïðèìåíåíèÿ õðîìàòîãðàôè÷åñêèõ êîëîíîê ñ àìèíî- è äèîëüíûìè ñîðáåíòàìè äëÿ ðàçäåëåíèÿ ñìåñåé à Êè ìî÷åâèíû
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    . Öåëü ðàáîòû— èññëåäîâàíèå âîçìîæíîñòè ïðèìåíåíèÿ æèäêîñòíîé õðîìàòîãðàôèè ãèäðîôèëüíûõ âçàèìîäåéñòâèé (Hydrophilic Interaction Liquid Chromatography; HILIC) äëÿ ðàçäåëåíèÿ à Êè ìî÷åâèíû íà õðîìàòîãðàôè÷åñêîé êîëîíêå ñ íèòðèëüíûì ñîðáåíòîì.

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Osipov AS, Nechaeva EB, Pobedin OA. The use of column chromatography with diol sorbent for analysis of diesel platinum coordination compounds. Himiko-farmatsevticheskiy zhurnal 2013;47(6): 51–3 (in Russian).
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    Ïåðåä ââåäåíèåì â õðîìàòîãðàô âñå ïðîáû öåíòðèôóãèðîâàëè ïðè 11 òûñ. îá/ìèí â òå÷åíèå 7 ìèí. ÐÅÇÓËÜÒÀÒÛ È ÎÁÑÓÆÄÅÍÈÅ Â óñëîâèÿõ æèäêîñòíîé õðîìàòîãðàôèè ãèäðîôèëüíûõ âçàèìîäåéñòâèé ñâîéñòâà êîëîíîê ñ íèòðèëüíûìè ñîðáåíòàìè ìîãóò áûòü, â çàâèñèìîñòè îò àíàëèçèðóåìûõîáúåêòîâ,êàêáëèçêè
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    ,òàêèêàðäèíàëüíî îòëè÷àòüñÿ îò êîëîíîê ñ àìèíîñîðáåíòàìè [8].  òàáëèöå 1 ïðèâåäåíû íåêîòîðûå ðåçóëüòàòû õðîìàòîãðàôèðîâàíèÿ ìîäåëüíîé ñìåñè ñòàíäàðòíûõ îáðàçöîâ ìî÷åâèíû è ÃÊ. Óâåëè÷åíèå âðåìåí óäåðæèâàíèÿ ìî÷åâèíû è ÃÊ, à òàêæå óëó÷øåíèå èõ ðàçäåëåíèÿ ñ âîçðàñòàíèåì äîëè àöåòîíèòðèëà â ïîäâèæíîéôàçåóêàçûâàåò,÷òîíàäàííûõêîëîíêàõèìååò ìåñòî íîðìàëüíî-ôàçîâûé ìåõàíèçì ðàçäåëåíèÿ â Ïðèìåíåíèå õðîìàò

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Osipov AS, Nechaeva EB. The use of chromatographic columns with nitrile and phenyl sorbents for the analysis of coordination compounds of platinum. Himiko-farmatsevticheskiy zhurnal 2014;48(8): 45–8 (in Russian).
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    Ïåðåä ââåäåíèåì â õðîìàòîãðàô âñå ïðîáû öåíòðèôóãèðîâàëè ïðè 11 òûñ. îá/ìèí â òå÷åíèå 7 ìèí. ÐÅÇÓËÜÒÀÒÛ È ÎÁÑÓÆÄÅÍÈÅ Â óñëîâèÿõ æèäêîñòíîé õðîìàòîãðàôèè ãèäðîôèëüíûõ âçàèìîäåéñòâèé ñâîéñòâà êîëîíîê ñ íèòðèëüíûìè ñîðáåíòàìè ìîãóò áûòü, â çàâèñèìîñòè îò àíàëèçèðóåìûõîáúåêòîâ,êàêáëèçêè
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    ,òàêèêàðäèíàëüíî îòëè÷àòüñÿ îò êîëîíîê ñ àìèíîñîðáåíòàìè [8].  òàáëèöå 1 ïðèâåäåíû íåêîòîðûå ðåçóëüòàòû õðîìàòîãðàôèðîâàíèÿ ìîäåëüíîé ñìåñè ñòàíäàðòíûõ îáðàçöîâ ìî÷åâèíû è ÃÊ. Óâåëè÷åíèå âðåìåí óäåðæèâàíèÿ ìî÷åâèíû è ÃÊ, à òàêæå óëó÷øåíèå èõ ðàçäåëåíèÿ ñ âîçðàñòàíèåì äîëè àöåòîíèòðèëà â ïîäâèæíîéôàçåóêàçûâàåò,÷òîíàäàííûõêîëîíêàõèìååò ìåñòî íîðìàëüíî-ôàçîâûé ìåõàíèçì ðàçäåëåíèÿ â Ïðèìåíåíèå õðîìàò

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Osipov AS, Nechaeva EB, Mironova MM, Kovaleva EL. The use of liquid chromatography of hydrophilic interactions for separation of butylhydroxyanisole isomers. Himiko-farmatsevticheskiy zhurnal 2015; 49(3): 50–2 (in Russian). AUTHORS
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    ÐÅÇÓËÜÒÀÒÛ È ÎÁÑÓÆÄÅÍÈÅ Â óñëîâèÿõ æèäêîñòíîé õðîìàòîãðàôèè ãèäðîôèëüíûõ âçàèìîäåéñòâèé ñâîéñòâà êîëîíîê ñ íèòðèëüíûìè ñîðáåíòàìè ìîãóò áûòü, â çàâèñèìîñòè îò àíàëèçèðóåìûõîáúåêòîâ,êàêáëèçêè[6, 7],òàêèêàðäèíàëüíî îòëè÷àòüñÿ îò êîëîíîê ñ àìèíîñîðáåíòàìè
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    .  òàáëèöå 1 ïðèâåäåíû íåêîòîðûå ðåçóëüòàòû õðîìàòîãðàôèðîâàíèÿ ìîäåëüíîé ñìåñè ñòàíäàðòíûõ îáðàçöîâ ìî÷åâèíû è ÃÊ. Óâåëè÷åíèå âðåìåí óäåðæèâàíèÿ ìî÷åâèíû è ÃÊ, à òàêæå óëó÷øåíèå èõ ðàçäåëåíèÿ ñ âîçðàñòàíèåì äîëè àöåòîíèòðèëà â ïîäâèæíîéôàçåóêàçûâàåò,÷òîíàäàííûõêîëîíêàõèìååò ìåñòî íîðìàëüíî-ôàçîâûé ìåõàíèçì ðàçäåëåíèÿ â Ïðèìåíåíèå õðîìàòîãðàôè÷åñêîé êîëîíêè ñ íèòðèëüíûì ñîðáåíòîì äëÿ àíàëèçà ãèäð